Anti-Diabetic Activity of Glycyrrhetinic Acid Derivatives FC-114 and FC-122: Scale-Up, In Silico, In Vitro, and In Vivo Studies


Por: Alvarez-Almazan, Samuel, Solis-Dominguez, Luz Cassandra, Duperou-Luna, Paulina, Fuerte-Gomez, Teresa, Gonzalez-Andrade, Martin, Aranda-Barradas, Maria E., Palacios-Espinosa, Juan Francisco, Perez-Villanueva, Jaime, Matadamas-Martinez, Felix, Miranda-Castro, Susana Patricia, Mercado-Marquez, Crisoforo, Cortes-Benitez, Francisco

Publicada: 1 ago 2023
Resumen:
Type 2 diabetes (T2D) is one of the most common diseases and the 8th leading cause of death worldwide. Individuals with T2D are at risk for several health complications that reduce their life expectancy and quality of life. Although several drugs for treating T2D are currently available, many of them have reported side effects ranging from mild to severe. In this work, we present the synthesis in a gram-scale as well as the in silico and in vitro activity of two semisynthetic glycyrrhetinic acid (GA) derivatives (namely FC-114 and FC-122) against Protein Tyrosine Phosphatase 1B (PTP1B) and a-glucosidase enzymes. Furthermore, the in vitro cytotoxicity assay on Human Foreskin fibroblast and the in vivo acute oral toxicity was also conducted. The anti-diabetic activity was determined in streptozotocin-induced diabetic rats after oral administration with FC-114 or FC-122. Results showed that both GA derivatives have potent PTP1B inhibitory activity being FC-122, a dual PTP1B/a-glucosidase inhibitor that could increase insulin sensitivity and reduce intestinal glucose absorption. Molecular docking, molecular dynamics, and enzymatic kinetics studies revealed the inhibition mechanism of FC-122 against a-glucosidase. Both GA derivatives were safe and showed better anti-diabetic activity in vivo than the reference drug acarbose. Moreover, FC-114 improves insulin levels while decreasing LDL and total cholesterol levels without decreasing HDL cholesterol.

Filiaciones:
Alvarez-Almazan, Samuel:
 Laboratory of Biotechnology, Unidad de Posgrado, Universidad Nacional Autónoma de México, Facultad de Estudios Superiores Cuautitlán Campus 1, Cuautitlán Izcalli, 54740, Mexico

Solis-Dominguez, Luz Cassandra:
 Laboratory of Biotechnology, Unidad de Posgrado, Universidad Nacional Autónoma de México, Facultad de Estudios Superiores Cuautitlán Campus 1, Cuautitlán Izcalli, 54740, Mexico

Duperou-Luna, Paulina:
 Laboratory of Synthesis and Isolation of Bioactive Substances, Departamento de Sistemas Biológicos, División de Ciencias Biológicas y de la Salud, Universidad Autónoma Metropolitana–Xochimilco (UAM–X), Mexico City, 04960, Mexico

Fuerte-Gomez, Teresa:
 Laboratory of Biotechnology, Unidad de Posgrado, Universidad Nacional Autónoma de México, Facultad de Estudios Superiores Cuautitlán Campus 1, Cuautitlán Izcalli, 54740, Mexico

Gonzalez-Andrade, Martin:
 Laboratory of Biosensors and Molecular Modelling, Departamento de Bioquímica, Facultad de Medicina, Universidad Nacional Autónoma de México, Mexico City, 04510, Mexico

Aranda-Barradas, Maria E.:
 Laboratory of Biotechnology, Unidad de Posgrado, Universidad Nacional Autónoma de México, Facultad de Estudios Superiores Cuautitlán Campus 1, Cuautitlán Izcalli, 54740, Mexico

Palacios-Espinosa, Juan Francisco:
 Laboratory of Synthesis and Isolation of Bioactive Substances, Departamento de Sistemas Biológicos, División de Ciencias Biológicas y de la Salud, Universidad Autónoma Metropolitana–Xochimilco (UAM–X), Mexico City, 04960, Mexico

Perez-Villanueva, Jaime:
 Laboratory of Synthesis and Isolation of Bioactive Substances, Departamento de Sistemas Biológicos, División de Ciencias Biológicas y de la Salud, Universidad Autónoma Metropolitana–Xochimilco (UAM–X), Mexico City, 04960, Mexico

Matadamas-Martinez, Felix:
 Laboratory of Synthesis and Isolation of Bioactive Substances, Departamento de Sistemas Biológicos, División de Ciencias Biológicas y de la Salud, Universidad Autónoma Metropolitana–Xochimilco (UAM–X), Mexico City, 04960, Mexico

Miranda-Castro, Susana Patricia:
 Laboratory of Biotechnology, Unidad de Posgrado, Universidad Nacional Autónoma de México, Facultad de Estudios Superiores Cuautitlán Campus 1, Cuautitlán Izcalli, 54740, Mexico

Mercado-Marquez, Crisoforo:
 Isolation and Animal Facility Unit, Facultad de Estudios Superiores Cuautitlán 28, Universidad Nacional Autónoma de México, Cuautitlán Izcalli, 54714, Mexico

Cortes-Benitez, Francisco:
 Laboratory of Synthesis and Isolation of Bioactive Substances, Departamento de Sistemas Biológicos, División de Ciencias Biológicas y de la Salud, Universidad Autónoma Metropolitana–Xochimilco (UAM–X), Mexico City, 04960, Mexico
ISSN: 16616596





INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES
Editorial
MDPI AG, POSTFACH, CH-4005 BASEL, SWITZERLAND, Suiza
Tipo de documento: Article
Volumen: 24 Número: 16
Páginas:
WOS Id: 001057280700001
ID de PubMed: 37628991
imagen gold, Gold